Table 1: Distillation Data TableGlasswareMass (g)BEFORE DISTILLATION Distillation Flask + boiling chips44.1161 gDistillation Flask + boiling chips + Unknown Liquid Mixture61.9474 gReceiving Flask30.2201 gAFTER DISTILLATION Receiving Flask + Low BP Liquid36.5895 gDistillation Flask + boiling chips + High BP Liquid54.8759 gDENSITY MEASUREMENT Volumetric Flask for LBP liquid (empty)17.2148 gVolumetric Density Flask + LBP liquid18.0846 gVolumetric Flask for HBP liquid (empty)14.5110 gVolumetric Flask + HBP liquid15.3117 gAdditional Calculated DataMass of the Unknown Liquid Mixture: 17.8271 gVapor temperature stabilized range for the LBP: 56–57°CLBP liquid mass: 6.3754 gHBP liquid mass: 10.9546 gBoiling point for LBP liquid: 66.1–66.3°CBoiling point for HBP liquid: 90.6–91.2°CLBP liquid density: 0.870 g/mLHBP liquid density: 0.801 g/mL Table 2: Solids Recovery and Melting Point DataGlasswareMass (g)Vial + Cap (for Crude Organic solid)18.0682 gVial + Cap + Crude Organic solid23.7049 gVial + Cap (for Crude Aqueous solid)18.1608 gVial + Cap + Crude Aqueous solid18.7765 gVial + Cap (for Pure Organic solid)44.4500 gVial + Cap + Pure Organic solid48.9147 gVial + Cap (for Pure Aqueous solid)75.5270 gVial + Cap + Pure Aqueous solid75.7302 gUnknown solid X: 21Mass of Crude Organic Solid (R–Z): 5.6942 g (Lab 3)Mass of Crude Aqueous Solid (R–CO2H): 0.6157 g (Lab 3)Mass of Pure Organic Solid (R–Z): 4.4638 g (Lab 4)Mass of Pure Aqueous Solid (R–CO2H): 0.2032 g (Lab 4)Melting Point Data (°C)Crude Organic Solid (R–Z): 23.6–44.5°CCrude Aqueous Solid (R–CO2H): 90.1–124.0°CPure Organic Solid (R–Z): 35.2–41.5°CPure Aqueous Solid (R–CO2H): 106.8–126.6°CUsing this data help me create four tables using the images attached this is not a graded assignment I just need help to study for my exam These tables MUST be included in the report for each of your unknowns in the ResultsSection (4 tables in total):Chemical Name:Percent RecoverySolidsMelting Point Data (°C)Unknown Code:Crude:Pure:Trial 1Trial 2AverageCrudePurePhysical AppearanceMS DataMolecular FormulaIHDM+ (m/z)Base Peak (m/z)Lost Fragments /Other Peaks (m/z)IR DataAbsorption Band1Wavenumber (cm³¹)IntensityShape234 (etc.)1H NMR DataProton(s)ABCD (etc.)13C NMRCarbon(s)1234 (etc.)Structure:8 (ppm)SplittingIntegration8 (ppm) CHE231LAQ22part of your references. You need to use at least 3 references for your lab report. The ACS styleguidelines can be found here: http://pubs.acs.org/isbn/97808412399999. Appendices:a. Spectra: You should only include both you 'H and 13C NMR spectra for the final report. MSand IR spectra does not have to be included. NMR spectra are typically given a Figure numberand a descriptive title (e.g. Figure 3. H NMR Spectrum of Liquid Unknown 11 (Diethyl ether)),and any important peaks can be labeled. On an NMR spectrum, include a structuralrepresentation of your molecule, indicating which hydrogens/carbons are represented by peaksA, B, C, etc. For example:Figure 3. 'H NMR Spectrum of Liquid Unknown 11 (diethyl ether)BA A10T6HPM-00-19587B6AB543210ppmb. Calculations: Include one example of the most important calculations performed during thewet labs (ex. percent recovery). Do not write each single percent recovery you performed.

Step 1: Physical ObservationThe compound identified as ethoxyethane (diethyl ether) was observed as…

These tables MUST be included in the report for each of your unknowns in the Results Section (4 tables in total): Chemical Name: Percent Recovery Solids Melting Point Data (°C) Unknown Code: Crude: Pure: Trial 1 Trial 2 Average Crude Pure Physical Appearance MS Data Molecular Formula IHD M+ (m/z) Base Peak (m/z) Lost Fragments / Other Peaks (m/z) IR Data Absorption Band 1 Wavenumber (cm³¹) Intensity Shape 2 3 4 (etc.) 1H NMR Data Proton(s) A B C D (etc.) 13C NMR Carbon(s) 1 2 3 4 (etc.) Structure: 8 (ppm) Splitting Integration 8 (ppm) CHE231L AQ22 part of your references. You need to use at least 3 references for your lab report. The ACS style guidelines can be found here: http://pubs.acs.org/isbn/9780841239999 9. Appendices: a. Spectra: You should only include both you 'H and 13C NMR spectra for the final report. MS and IR spectra does not have to be included. NMR spectra are typically given a Figure number and a descriptive title (e.g. Figure 3. H NMR Spectrum of Liquid Unknown 11 (Diethyl ether)), and any important peaks can be labeled. On an NMR spectrum, include a structural representation of your molecule, indicating which hydrogens/carbons are represented by peaks A, B, C, etc. For example: Figure 3. 'H NMR Spectrum of Liquid Unknown 11 (diethyl ether) B A A 10 T 6 HPM-00-195 8 7 B 6 A B 5 4 3 2 1 0 ppm b. Calculations: Include one example of the most important calculations performed during the wet labs (ex. percent recovery). Do not write each single percent recovery you performed.

2nd Edition

ISBN:9781285686691

Author:Crouch

Publisher:Crouch

Chapter3: Statistical Tests With Excel

Section: Chapter Questions

Problem 4P

Related questions

Question

Table 1: Distillation Data Table

Glassware	Mass (g)
BEFORE DISTILLATION
Distillation Flask + boiling chips	44.1161 g
Distillation Flask + boiling chips + Unknown Liquid Mixture	61.9474 g
Receiving Flask	30.2201 g
AFTER DISTILLATION
Receiving Flask + Low BP Liquid	36.5895 g
Distillation Flask + boiling chips + High BP Liquid	54.8759 g
DENSITY MEASUREMENT
Volumetric Flask for LBP liquid (empty)	17.2148 g
Volumetric Density Flask + LBP liquid	18.0846 g
Volumetric Flask for HBP liquid (empty)	14.5110 g
Volumetric Flask + HBP liquid	15.3117 g

Additional Calculated Data

Table 2: Solids Recovery and Melting Point Data

Glassware	Mass (g)
Vial + Cap (for Crude Organic solid)	18.0682 g
Vial + Cap + Crude Organic solid	23.7049 g
Vial + Cap (for Crude Aqueous solid)	18.1608 g
Vial + Cap + Crude Aqueous solid	18.7765 g
Vial + Cap (for Pure Organic solid)	44.4500 g
Vial + Cap + Pure Organic solid	48.9147 g
Vial + Cap (for Pure Aqueous solid)	75.5270 g
Vial + Cap + Pure Aqueous solid	75.7302 g